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首頁» 過刊瀏覽» 2024» Vol.9» lssue(2) 196-212???? DOI : 10.3969/j.issn.2096-1693.2024.02.015
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川東北地區(qū)侏羅系涼高山組頁巖儲集空間特征及頁巖油可動性探索
楊鑫翊, 王民, 白雪峰, 王鑫, 應玉雙, 李天一, 董景海, 黃世偉, 陳俊陽
1 深層油氣全國重點實驗室( 中國石油大學( 華東)),,青島 266580 2 中國石油大學( 華東) 地球科學與技術學院,,青島 266580 3 大慶油田有限責任公司勘探開發(fā)研究院,,大慶 163712 4 大慶油田有限責任公司勘探事業(yè)部,大慶 163453
Reservoir space characteristics and exploration of shale oil mobility of the Jurassic Lianggaoshan Formation shale in the northeastern Sichuan Basin
YANG Xinyi, WANG Min, BAI Xuefeng, WANG Xin, YING Yushuang, LI Tianyi, DONG Jinghai, HUANG Shiwei, CHEN Junyang
1 State Key Laboratory of Deep Oil and Gas, China University of Petroleum-East China, Qingdao 266580, China 2 School of Geosciences, China University of Petroleum-East China, Qingdao 266580, China 3 Exploration and Development Research Institute, Daqing Oil field Company Limited, Daqing 163712, China 4 Exploration Department, Daqing Oil field Company Limited, Daqing 163453, China

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摘要? 侏羅系涼高山組頁巖是四川盆地重點勘探層段,,但其孔隙結(jié)構(gòu)與頁巖油可動性尚不明晰,。為揭示川東北地區(qū)侏羅系涼高山組頁巖儲集空間特征及頁巖油可動性,本文依據(jù)沉積構(gòu)造和礦物組成劃分巖相類型,,開展總有機碳測定,、巖石熱解和鏡質(zhì)體反射率實驗獲取基礎地化特征;利用場發(fā)射掃描電鏡,、核磁共振,、低溫氮氣吸附、高壓壓汞手段實現(xiàn)孔隙度,、孔隙結(jié)構(gòu)的表征及評價,,并對比不同巖相間儲集空間特征差異;在離心時間為3 h,,離心轉(zhuǎn)速為11 000 r/min條件下,,開展核磁-離心定量評價不同巖相頁巖油可動性,并明確影響因素,,建立可動油量測井評價模型并選出有利巖相,。結(jié)果表明:(1)川東北地區(qū)涼高山組頁巖總有機碳含量主要分布在0.15%~2.95%之間,Ro值介于1.06%~1.68%之間,,處于成熟-高熟階段,;輕烴恢復后,S1 分布范圍為0.03~3.32 mg/g,;礦物類型以黏土礦物和石英為主,,發(fā)育的巖相類型為紋層狀黏土質(zhì)頁巖相、紋層狀長英質(zhì)頁巖相,、層狀混合質(zhì)頁巖相和塊狀粉砂質(zhì)泥巖相,。(2)頁巖儲集空間主要發(fā)育黏土礦物晶間孔、有機孔,,另外可見石英溶蝕孔,、粒間孔、黃鐵礦晶間孔和微裂縫,;孔隙度介于1.15%~4.71%,;頁巖孔徑分布范圍較寬,孔體積主要由介孔和小于200 nm的宏孔貢獻,紋層狀黏土質(zhì)頁巖儲集物性較好,。(3)涼高山組頁巖可動油量分布在0.25~3.26 mg/g,,可動油率分布在5.13%~44.83%,,紋層狀黏土質(zhì)頁巖可動性較好,,塊狀粉砂質(zhì)泥巖可動性較差;TOC,、黏土礦物含量和孔隙度是控制涼高山組頁巖油可動性的主要因素,,利用這3 個因素建立并驗證了可動油量預測模型,優(yōu)選出紋層狀黏土質(zhì)頁巖為涼高山組重點勘探對象,,對四川盆地頁巖油的勘探開發(fā)具有指示意義,。
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關鍵詞 : 四川盆地,涼高山組,頁巖油,可動性,定量預測模型
Abstract

The Jurassic Lianggaoshan Formation shale is a key exploration interval in the Sichuan Basin, but its pore structure and shale oil mobility are still unclear. In order to reveal the reservoir space characteristics and the mobility of shale oil in the Lianggaoshan Formation, this paper divided lithofacies types according to sedimentary structure and mineral composition. Basic geochemical characteristics were obtained by total organic carbon determination, rock pyrolysis and vitrinite reflectance experiments. The porosity and pore structure were characterized and evaluated by means of field emission scanning electron microscopy, nuclear magnetic resonance, low temperature nitrogen adsorption and high pressure mercury injection. The difference in reservoir space characteristics between different rock phases was also compared. With a centrifugation time of 3 h and centrifugation speed of 11 000 r/min, quantitative evaluation of the mobility of shale oil with different lithofacies was carried out by NMR centrifugation and the influential factors are clearly defined. The evaluation model of movable oil quantity logging was established and. the favorable rock facies was selected. The results show that: (1) The TOC of Lianggaoshan Formation shale is mainly between 0.15%~2.95%, the Ro is between 1.06%~1.68%, and the shale is in the mature-high mature stage. After the recovery of light hydrocarbons, the change range of S1 was 0.03 mg/g ~3.32 mg/g. The mineral types are mainly clay minerals and quartz. The developed lithofacies are lamellar clay shale facies, lamellar felsic shale facies, lamellar mixed shale facies and massive silty mudstone facies. (2) Shale reservoir space types are mainly clay mineral intergranular pores, organic matter pores, in addition to quartz dissolution pores, interparticle pores, pyrite intergranular pores and microfractures. The porosity is between 1.15% and 4.71%. The shale has a wide pore size distribution. The pore volume is mainly contributed by mesopores and macropores smaller than 200 nm. Laminated clay shale has the best physical properties (3) the movable oil content of the Lianggaoshan Formation shale ranges from 0.25 mg/g to 3.26 mg/g, and the movable oil rate ranges from 5.13% to 44.8%. Lamellar clay shale has the best mobility, and massive silty mudstone has the worst mobility. TOC, clay mineral content and porosity are the key factors controlling movable oil content in the Lianggaoshan Formation. Based on these three factors, a mobile oil quantity prediction model is established and verified. Laminated clayey shale is preferred as the key exploration object of the Lianggaoshan Formation, which is indicative of the exploration and development of shale oil in the Sichuan Basin.


Key words: Sichuan Basin; Lianggaoshan Formation; shale oil; mobility; quantitative estimation model
收稿日期: 2024-04-30 ????
PACS: ? ?
基金資助:國家自然科學基金項目(41922015,、 42072147、 42102154) 聯(lián)合資助
通訊作者: wangm@upc.edu.cn
引用本文: ??
楊鑫翊, 王民, 白雪峰, 王鑫, 應玉雙, 李天一, 董景海, 黃世偉, 陳俊陽. 川東北地區(qū)侏羅系涼高山組頁巖儲集空間特征及頁巖油 可動性探索. 石油科學通報, 2024, 02: 196-212 YANG Xinyi, WANG Min, BAI Xuefeng, WANG Xin, YING Yushuang, LI Tianyi, DONG Jinghai, HUANG Shiwei, CHEN Junyang. Reservoir space characteristics and exploration of shale oil mobility of the Jurassic Lianggaoshan Formation shale in the northeastern Sichuan Basin. Petroleum Science Bulletin, 2024, 02: 196-212.
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