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首頁(yè)» 過(guò)刊瀏覽» 2024» Vol.9» lssue(2) 196-212???? DOI : 10.3969/j.issn.2096-1693.2024.02.015
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川東北地區(qū)侏羅系涼高山組頁(yè)巖儲(chǔ)集空間特征及頁(yè)巖油可動(dòng)性探索
楊鑫翊, 王民, 白雪峰, 王鑫, 應(yīng)玉雙, 李天一, 董景海, 黃世偉, 陳俊陽(yáng)
1 深層油氣全國(guó)重點(diǎn)實(shí)驗(yàn)室( 中國(guó)石油大學(xué)( 華東)),,青島 266580 2 中國(guó)石油大學(xué)( 華東) 地球科學(xué)與技術(shù)學(xué)院,,青島 266580 3 大慶油田有限責(zé)任公司勘探開(kāi)發(fā)研究院,,大慶 163712 4 大慶油田有限責(zé)任公司勘探事業(yè)部,,大慶 163453
Reservoir space characteristics and exploration of shale oil mobility of the Jurassic Lianggaoshan Formation shale in the northeastern Sichuan Basin
YANG Xinyi, WANG Min, BAI Xuefeng, WANG Xin, YING Yushuang, LI Tianyi, DONG Jinghai, HUANG Shiwei, CHEN Junyang
1 State Key Laboratory of Deep Oil and Gas, China University of Petroleum-East China, Qingdao 266580, China 2 School of Geosciences, China University of Petroleum-East China, Qingdao 266580, China 3 Exploration and Development Research Institute, Daqing Oil field Company Limited, Daqing 163712, China 4 Exploration Department, Daqing Oil field Company Limited, Daqing 163453, China

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摘要? 侏羅系涼高山組頁(yè)巖是四川盆地重點(diǎn)勘探層段,但其孔隙結(jié)構(gòu)與頁(yè)巖油可動(dòng)性尚不明晰,。為揭示川東北地區(qū)侏羅系涼高山組頁(yè)巖儲(chǔ)集空間特征及頁(yè)巖油可動(dòng)性,,本文依據(jù)沉積構(gòu)造和礦物組成劃分巖相類(lèi)型,開(kāi)展總有機(jī)碳測(cè)定,、巖石熱解和鏡質(zhì)體反射率實(shí)驗(yàn)獲取基礎(chǔ)地化特征,;利用場(chǎng)發(fā)射掃描電鏡、核磁共振,、低溫氮?dú)馕?、高壓壓汞手段?shí)現(xiàn)孔隙度,、孔隙結(jié)構(gòu)的表征及評(píng)價(jià),并對(duì)比不同巖相間儲(chǔ)集空間特征差異,;在離心時(shí)間為3 h,,離心轉(zhuǎn)速為11 000 r/min條件下,開(kāi)展核磁-離心定量評(píng)價(jià)不同巖相頁(yè)巖油可動(dòng)性,,并明確影響因素,,建立可動(dòng)油量測(cè)井評(píng)價(jià)模型并選出有利巖相。結(jié)果表明:(1)川東北地區(qū)涼高山組頁(yè)巖總有機(jī)碳含量主要分布在0.15%~2.95%之間,,Ro值介于1.06%~1.68%之間,,處于成熟-高熟階段;輕烴恢復(fù)后,,S1 分布范圍為0.03~3.32 mg/g,;礦物類(lèi)型以黏土礦物和石英為主,發(fā)育的巖相類(lèi)型為紋層狀黏土質(zhì)頁(yè)巖相,、紋層狀長(zhǎng)英質(zhì)頁(yè)巖相,、層狀混合質(zhì)頁(yè)巖相和塊狀粉砂質(zhì)泥巖相。(2)頁(yè)巖儲(chǔ)集空間主要發(fā)育黏土礦物晶間孔,、有機(jī)孔,另外可見(jiàn)石英溶蝕孔,、粒間孔,、黃鐵礦晶間孔和微裂縫;孔隙度介于1.15%~4.71%,;頁(yè)巖孔徑分布范圍較寬,,孔體積主要由介孔和小于200 nm的宏孔貢獻(xiàn),紋層狀黏土質(zhì)頁(yè)巖儲(chǔ)集物性較好,。(3)涼高山組頁(yè)巖可動(dòng)油量分布在0.25~3.26 mg/g,,可動(dòng)油率分布在5.13%~44.83%,紋層狀黏土質(zhì)頁(yè)巖可動(dòng)性較好,,塊狀粉砂質(zhì)泥巖可動(dòng)性較差,;TOC、黏土礦物含量和孔隙度是控制涼高山組頁(yè)巖油可動(dòng)性的主要因素,,利用這3 個(gè)因素建立并驗(yàn)證了可動(dòng)油量預(yù)測(cè)模型,,優(yōu)選出紋層狀黏土質(zhì)頁(yè)巖為涼高山組重點(diǎn)勘探對(duì)象,對(duì)四川盆地頁(yè)巖油的勘探開(kāi)發(fā)具有指示意義,。
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關(guān)鍵詞 : 四川盆地,涼高山組,頁(yè)巖油,可動(dòng)性,定量預(yù)測(cè)模型
Abstract

The Jurassic Lianggaoshan Formation shale is a key exploration interval in the Sichuan Basin, but its pore structure and shale oil mobility are still unclear. In order to reveal the reservoir space characteristics and the mobility of shale oil in the Lianggaoshan Formation, this paper divided lithofacies types according to sedimentary structure and mineral composition. Basic geochemical characteristics were obtained by total organic carbon determination, rock pyrolysis and vitrinite reflectance experiments. The porosity and pore structure were characterized and evaluated by means of field emission scanning electron microscopy, nuclear magnetic resonance, low temperature nitrogen adsorption and high pressure mercury injection. The difference in reservoir space characteristics between different rock phases was also compared. With a centrifugation time of 3 h and centrifugation speed of 11 000 r/min, quantitative evaluation of the mobility of shale oil with different lithofacies was carried out by NMR centrifugation and the influential factors are clearly defined. The evaluation model of movable oil quantity logging was established and. the favorable rock facies was selected. The results show that: (1) The TOC of Lianggaoshan Formation shale is mainly between 0.15%~2.95%, the Ro is between 1.06%~1.68%, and the shale is in the mature-high mature stage. After the recovery of light hydrocarbons, the change range of S1 was 0.03 mg/g ~3.32 mg/g. The mineral types are mainly clay minerals and quartz. The developed lithofacies are lamellar clay shale facies, lamellar felsic shale facies, lamellar mixed shale facies and massive silty mudstone facies. (2) Shale reservoir space types are mainly clay mineral intergranular pores, organic matter pores, in addition to quartz dissolution pores, interparticle pores, pyrite intergranular pores and microfractures. The porosity is between 1.15% and 4.71%. The shale has a wide pore size distribution. The pore volume is mainly contributed by mesopores and macropores smaller than 200 nm. Laminated clay shale has the best physical properties (3) the movable oil content of the Lianggaoshan Formation shale ranges from 0.25 mg/g to 3.26 mg/g, and the movable oil rate ranges from 5.13% to 44.8%. Lamellar clay shale has the best mobility, and massive silty mudstone has the worst mobility. TOC, clay mineral content and porosity are the key factors controlling movable oil content in the Lianggaoshan Formation. Based on these three factors, a mobile oil quantity prediction model is established and verified. Laminated clayey shale is preferred as the key exploration object of the Lianggaoshan Formation, which is indicative of the exploration and development of shale oil in the Sichuan Basin.


Key words: Sichuan Basin; Lianggaoshan Formation; shale oil; mobility; quantitative estimation model
收稿日期: 2024-04-30 ????
PACS: ? ?
基金資助:國(guó)家自然科學(xué)基金項(xiàng)目(41922015,、 42072147,、 42102154) 聯(lián)合資助
通訊作者: [email protected]
引用本文: ??
楊鑫翊, 王民, 白雪峰, 王鑫, 應(yīng)玉雙, 李天一, 董景海, 黃世偉, 陳俊陽(yáng). 川東北地區(qū)侏羅系涼高山組頁(yè)巖儲(chǔ)集空間特征及頁(yè)巖油 可動(dòng)性探索. 石油科學(xué)通報(bào), 2024, 02: 196-212 YANG Xinyi, WANG Min, BAI Xuefeng, WANG Xin, YING Yushuang, LI Tianyi, DONG Jinghai, HUANG Shiwei, CHEN Junyang. Reservoir space characteristics and exploration of shale oil mobility of the Jurassic Lianggaoshan Formation shale in the northeastern Sichuan Basin. Petroleum Science Bulletin, 2024, 02: 196-212.
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