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首頁» 過刊瀏覽» 2021» Vol.6» Issue(1) 46-57???? DOI : 10.3969/j.issn.2096-1693.2021.01.004
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模擬退火法結合兩點簇函數(shù)重構與表征頁巖有機質各向異性
隋微波,尤園 ,程思,鄭衣珍
1 中國石油大學(北京) 石油工程學院,北京 102249 2 中國石油大學(北京) 油氣資源與探測國家重點實驗室,北京 102249
Reconstructing and characterizing the anisotropy of shale organic matter with a two-point cluster function and a simulated annealing method
SUI Weibo, YOU Yuan, CHENG Si, ZHENG Yizhen
1 College of Petroleum Engineering, China University of Petroleum-Beijing, Beijing 102249, China 2 State Key Laboratory of Petroleum Resources and Prospecting, China University of Petroleum-Beijing, Beijing 102249, China

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摘要? 頁巖有機質及其孔隙分布與頁巖吸附氣含量和氣體微觀滲流機理密切相關,研究表明頁巖中有機質分布 在孔隙尺度下具有各向異性特征,然而現(xiàn)有的頁巖數(shù)字巖心重構算法未能對該特征進行有效描述。本文針對頁 巖樣品中有機質分布的各向異性特征,提出在數(shù)字巖心傳統(tǒng)模擬退火數(shù)值重構方法基礎上引進兩點簇函數(shù)作為 表征有機質分布連續(xù)性的統(tǒng)計指示函數(shù)。兩點簇函數(shù)雖然屬于兩點概率函數(shù),但是含有高階結構信息,因此兩 點簇函數(shù)較之兩點相關函數(shù)是對結構變化敏感性更強的統(tǒng)計指示函數(shù)。本文介紹了耦合兩點簇函數(shù)的模擬退火 算法模型,并以四川盆地下志留系龍馬溪組頁巖巖心樣品為例詳細論述了“樣品成像—圖像處理—函數(shù)提取— 重構計算”的系統(tǒng)性方法流程。研究通過場發(fā)射掃描電鏡實驗和聚焦離子束—場發(fā)射掃描電鏡實驗和圖像處理, 獲得了孔隙尺度下的頁巖有機質及其孔隙分布,并從中提取了巖心樣品在三個正交方向的統(tǒng)計關聯(lián)函數(shù)包括單 點相關函數(shù)、兩點相關函數(shù)、線性路徑函數(shù)和兩點簇函數(shù)。論文建立了有機質團塊三維重構的有效方法,并將 以上統(tǒng)計關聯(lián)函數(shù)應用于“雙重區(qū)域”模擬退火法重構過程,分別獲得有機質、有機質孔隙和基質孔隙的重構 模型,通過將三者耦合獲得頁巖樣品最終的數(shù)字巖心三維重構模型。重構頁巖數(shù)字巖心三個正交方向的兩點簇 函數(shù)分布曲線表明有機質具有明顯的各向異性。通過比較真實頁巖樣品與重構頁巖數(shù)字巖心的有機質等體積半 徑分布、有機質面積、有機質延伸率等參數(shù)分布,證明了兩點簇函數(shù)方法表征頁巖有機質各向異性分布特征的 有效性,該方法可應用于頁巖數(shù)字巖心重構的相關研究工作中。
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關鍵詞 : 頁巖;數(shù)字巖心;有機質孔隙;兩點簇函數(shù);各向異性;模擬退火法
Abstract
Organic matter and its pore distribution are closely related to the adsorbed gas content of shale and the microscopic    gas flow mechanism. Studies have shown that the organic matter distribution in shale has anisotropic characteristics at the pore    scale. However, the existing digital core reconstruction algorithms for shale cannot effectively describe this feature. Aiming at    the anisotropic characteristics of organic matter distribution in shale samples, this paper introduced a two-point cluster function    as a statistical indicator to characterize the continuity of organic matter distribution based on the traditional simulated numerical    annealing reconstruction method for digital cores. Although the two-point cluster function belongs to the two-point probability    
function, it contains high-order structural information. Therefore, the two-point cluster function is a statistical indicator that is    more sensitive to structural changes than the two-point correlation function. This paper presented the mathematical model of the    simulated annealing method coupled with a two-point cluster function. Meanwhile, taking the shale core sample of the Longmaxi    Formation of the Lower Silurian in the Sichuan Basin as an example, the systematic method flow of "sample imaging?image    processing?function extraction?reconstruction calculation" was discussed in detail. Through field emission scanning electron    microscopy (FESEM) and focused ion beam-field emission scanning electron microscopy (FIB-SEM) and image processing, the    shale organic matter and its pore distribution at the pore scale were obtained, and the statistical correlation of core samples in    three orthogonal directions was extracted. Functions include a single-point correlation function, two-point correlation function,    linear path function and a two-point cluster function. The paper established an effective method for three-dimensional recon   struction of organic matter aggregates, and applied the above statistical correlation functions to the reconstruction process of the    Dual-Region simulated annealing method to obtain reconstruction models of organic matter, organic matter pores and matrix    pores respectively. Combining the three coupled regions produces the final digital core 3D reconstruction model of the shale    sample. The reconstruction of the two-point cluster function distribution curve in three orthogonal directions of the shale digital    core shows that the organic matter has obvious anisotropy. By comparing organic matter equivalent volume radius distribution,    organic matter area, organic matter elongation and other parameter distributions of real shale samples and reconstructed shale    digital cores, the validity of the two-point cluster function method to characterize the anisotropic distribution of shale organic    matter has been proved. This method can be applied to related research work on shale digital core reconstruction.  


Key words: shale; digital core; organic matter; two-point cluster function; anisotropy; simulated annealing method
收稿日期: 2021-03-31 ????
PACS: ? ?
基金資助:國家自然科學基金面上項目(51474224) 資助
通訊作者: [email protected]
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SUI Weibo, YOU Yuan, CHENG Si, ZHENG Yizhen. Reconstructing and characterizing the anisotropy of shale organic matter with a two-point cluster function and a simulated annealing method. Petroleum Science Bulletin, 2021, 01: 46-57.
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