本中心成立于2004年,是中國石油大學(xué)(北京)重點(diǎn)建設(shè)的公共實(shí)驗(yàn)平臺(tái)之一,,現(xiàn)有大型儀器設(shè)備30余臺(tái)(套),。圍繞油品性質(zhì)、組成開展分析測(cè)試服務(wù)和基礎(chǔ)研究工作。
中心可承擔(dān)有機(jī)地球化學(xué)及石油化工領(lǐng)域的分析測(cè)試服務(wù),,如石油生物標(biāo)志化合物分析,、原油蒸餾及性質(zhì)分析、油品分子組成,、模擬蒸餾,、有機(jī)元素分析等測(cè)試任務(wù)。中心擁有一支較高技術(shù)素質(zhì)的檢測(cè)人員隊(duì)伍,,能夠滿足分析測(cè)試及研究開發(fā)的技術(shù)需要,。非常重視加快技術(shù)服務(wù)的響應(yīng)時(shí)間和提高工作效率,以滿足現(xiàn)代化科研工作的實(shí)際需要,。長(zhǎng)期為國內(nèi)外科研機(jī)構(gòu),、石油、石化企業(yè)提供優(yōu)質(zhì)高效的分析測(cè)試服務(wù),,大型儀器設(shè)備運(yùn)行狀況良好,,其中氣相色譜質(zhì)譜聯(lián)用儀入選“高等學(xué)校儀器設(shè)備和優(yōu)質(zhì)資源共享系統(tǒng)”,長(zhǎng)期承擔(dān)大量對(duì)外分析測(cè)試服務(wù),。
以大型儀器設(shè)備為依托,,分析測(cè)試中心圍繞重質(zhì)油組成化學(xué)開展深入研究,建立了一系列石油分子組成的分析方法,,從分子水平揭示重質(zhì)油,、煤液化產(chǎn)物、生物質(zhì)熱解油,、天然可溶有機(jī)物等復(fù)雜體系的化學(xué)組成,,不斷挑戰(zhàn)分析化學(xué)與石油化學(xué)的世界難題。

實(shí)驗(yàn)室整體布局

高分辨質(zhì)譜儀
取得成果:分析中心獨(dú)立完成的研究論文(2010-2012)
1. Zhou, X.; Shi, Q.; Zhang, Y.; Zhao, S.; Zhang, R.; Chung, K.H.; Xu, C. Analysis of saturated hydrocarbons by redox reaction with negative-ion electrospray Fourier transform ion cyclotron resonance mass spectrometry. Analytical Chemistry 2012, 84 (7), 3192-3199.
2. Long, H.; Shi, Q.; Pan, N.; Zhang, Y.; Cui, D.; Chung, K.H.; Zhao, S.; Xu, C. Characterization of middle-temperature gasification coal tar: 2. Neutral fraction by extrography followed by GC-MS and ESI FT-ICR MS.Energy & Fuels 2012.
3. Zhu, X.; Shi, Q.; Zhang, Y.; Pan, N.; Xu, C.; Chung, K.H.; Zhao, S. Characterization of nitrogen compounds in coker heavy gas oil and its subfractions by liquid chromatographic separation followed by Fourier transform ion cyclotron resonance mass spectrometry. Energy & Fuels 2011, 25 (1), 281-287.
4. Zhang, Y.; Shi, Q.; Li, A.; Chung, K.H.; Zhao, S.; Xu, C. Partitioning of crude oil acidic compounds into subfractions by extrography and identification of isoprenoidyl phenols and tocopherols. Energy & Fuels 2011, 25 (11), 5083-5089.
5. Zhang, Y.; Zhao, H.; Shi, Q.; Chung, K.H.; Zhao, S.; Xu, C. Molecular investigation of crude oil sludge from an electric dehydrator. Energy & Fuels 2011, 25 (7), 3116-3124.
6. Liu, P.; Shi, Q.; Pan, N.; Zhang, Y.; Chung, K.H.; Zhao, S.; Xu, C. Distribution of sulfides and thiophenic compounds in VGO subfractions: Characterized by positive-ion electrospray Fourier transform ion cyclotron resonance mass spectrometry. Energy & Fuels 2011, 25 (7), 3014-3020.
7. Zhang, Y.; Xu, C.; Shi, Q.; Zhao, S.; Chung, K.H.; Hou, D. Tracking neutral nitrogen compounds in subfractions of crude oil obtained by liquid chromatography separation using negative-ion electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry. Energy & Fuels 2010, 24 (12), 6321-6326.
8. Shi, Q.; Zhao, S.; Xu, Z.; Chung, K.H.; Zhang, Y.; Xu, C. Distribution of acids and neutral nitrogen compounds in a chinese crude oil and its fractions: Characterized by negative-ion electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry. Energy & Fuels 2010, 24 (7), 4005-4011.
9. Shi, Q.; Yan, Y.; Wu, X.; Li, S.; Chung, K.H.; Zhao, S.; Xu, C. Identification of dihydroxy aromatic compounds in a low-temperature pyrolysis coal tar by gas chromatography-mass spectrometry (GC-MS) and Fourier transform ion cyclotron resonance mass spectrometry (FT-ICR MS). Energy & Fuels 2010, 24 (10), 5533-5538.
10. Shi, Q.; Xu, C.; Zhao, S.; Chung, K.H.; Zhang, Y.; Gao, W. Characterization of basic nitrogen species in coker gas oils by positive-ion electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry. Energy & Fuels 2010, 24 (1), 563-569.
11. Shi, Q.; Pan, N.; Liu, P.; Chung, K.H.; Zhao, S.; Zhang, Y.; Xu, C. Characterization of sulfur compounds in oilsands bitumen by methylation followed by positive-ion electrospray ionization and Fourier transform ion cyclotron resonance mass spectrometry. Energy & Fuels 2010, 24 (5), 3014-3019.
12. Shi, Q.; Hou, D.; Chung, K.H.; Xu, C.; Zhao, S.; Zhang, Y. Characterization of heteroatom compounds in a crude oil and its saturates, aromatics, resins, and asphaltenes (SARA) and non-basic nitrogen fractions analyzed by negative-ion electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry. Energy & Fuels 2010, 24 (4), 2545-2553.
13. Liu, P.; Shi, Q.; Chung, K.H.; Zhang, Y.; Pan, N.; Zhao, S.; Xu, C. Molecular characterization of sulfur compounds in Venezuela crude oil and its SARA fractions by electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry. Energy & Fuels 2010, 24 (9), 5089-5096.
14. Liu, P.; Xu, C.; Shi, Q.; Pan, N.; Zhang, Y.; Zhao, S.; Chung, K.H. Characterization of sulfide compounds in petroleum: Selective oxidation followed by positive-ion electrospray Fourier transform ion cyclotron resonance mass spectrometry. Analytical Chemistry 2010, 82 (15), 6601-6606.